The proven design ensures very low backstreaming, reduced outgassing and minimized sealing requirements. All systems comprise oil diffusion pump, rotary vane backing pump, backing pressure gauge pia 1. It is used to produce vacuums in the range of 10e5 to 10e7 torr. Oil diffusion pump systems, dp complete, ready to use pumping system with a pillar design, for the production of high vacuum using oil diffusion principles.
The edwards diffstak vapour diffusion pumps are compact, watercooled pumps with integral cooled baffles which provide exceptionally clean pumping. Yet oil diffusion pumps require careful maintenance in order to maintain a high. It is also used in vapor ejector pumps that attain vacuum of 10e4 to 10e5 torr. This article will explain practical steps that can be taken to ensure optimal performance of.
Oil diffusion vacuum pump pfl series ulvac products. Inland vacuums silicone diffusion pump oils invoil 702, 704, and 705 are durable fluids designed for a variety of high vacuum applications and for fast pumping large volumes of gas. Oil diffusion pumps are still the most popular type of high vacuum pump because they are relatively inexpensive, highly reliable and very durable. Genuine oil ulvoil d series was developed specific for oil diffusion pumps and b6 was designed specific for oil diffusion ejector pumps. An oil diffusion pump backed by a rotary vane pump is by far the most common. The oil diffusion pump consists of a pump body, boiler heater and 3stage fractionating jet stack assembly. This advantage will allow the user to establish a homogenous vacuum system, which tends to eliminate the problems generally associated with the cross contamination of dissimilar fluids. Aug 14, 2014 oil diffusion pumps remain in popular use in the vacuum heat treating industry, possibly one of the few applications remaining for this type of high vacuum pump in the western world.
Maintaining oil diffusion pumps vacuum furnace engineering. Oil diffusion vacuum pump pfl series close attention to material selection and manufacturing techniques ensure reliable operation and a very low cost of ownership for the pfl series. The various oils also have different thermal breakdown temperatures the temperature at which the oil molecules break down and combine with any available. Oil diffusion pump ulkpflpbl series pbl series oil. All agilent diffusion pumps, 704 silicone oil 1 gallon. Even as turbomolecular vacuum pumps have displaced most small laboratory sized oil diffusion pumps these days because of perceived ease of use and cleanliness, most high vacuum heat treating furnaces still rely on a large oil diffusion pumps to generate the pressures below about 103 torr needed for many metal conditioning processes. Oil diffusion pumps are still the most popular type of highvacuum pump because they are relatively inexpensive, highly reliable and very durable. Please note that in these tips, we will use the terms oil and fluid. Methods for removing contaminants from diffusion pump silicone oil during operation and for reclaiming contaminated oil by highvacuum molecular distillation are. Inland vacuums silicone diffusion pump oils invoil 702, 704, and 705 are durable fluids designed for a variety of high vacuum applications and for. The diffusion pump uses the vapor of a boiling fluid to capture air molecules.
Mar 10, 2015 even as turbomolecular vacuum pumps have displaced most small laboratory sized oil diffusion pumps these days because of perceived ease of use and cleanliness, most high vacuum heat treating furnaces still rely on a large oil diffusion pumps to generate the pressures below about 103 torr needed for many metal conditioning processes. Typical properties of santovac 5 diffusion pump oil. Backstreaming of oil vapor in oil diffusion vacuum pumps. A vacuum of 103 torr has removed a great many of the atmospheric molecules, but this is actually the level at which a vacuum diffusion pump begins to operate. The oil diffusion pump is operated with an oil of low. Without a doubt, youll have questions on proper diffusion pump operation. The oil diffusion pumps are vibrationfree, reliable, and less expensive, while they may introduce contamination because of oil vapor. Since the diffusion pump cannot exhaust directly to atmospheric pressure, the fore pump is used to maintain proper discharge pressure conditions. Oil diffusion applications for oil diffusion pumps range from mass spectrometry and analytical instrumentation to nanotechology and research and development. At this point, the vacuum diffusion pump takes over to create a vacuum ranging from 103 to 109 mbar. High vacuum pump, diffusion pump, oil diffusion pumps. The diffusion vacuum pump construction consists of an oil boiler connected to a central multistage jet assembly.
Servovacuum vm 4 is a specially developed product having low vapour pressure 1 x 106 mm of hg at 200c and high thermal. The working uid oil is heated in the boiler, vaporized and streams out of each stage of the jet stack at high speed. Diffusion pump is an oilbased vacuum pump, that is used for obtaining different levels of vacuum even high vacuum of 10 powered 9 pascal. High vacuum oil diffusion pumps oil diffusion pumps are simple, robust and reliable high vacuum pumps with lowest initial and maintenance costs by far. Physics and engineering of high and very high vacuum, leningrad 1985, p. We specialize in offering high quality silicone diffusion pump oil backed by worldclass technical and customer support. The diffusion pump is the most common type of pump for use in high vacuum applications. It is very reliable and longlived, although when misused it can create a great deal of contamination in the processing chamber. Diffusion pump oil oil diffusion pumpvacuum pump vacuum. Select the optimal oil for your pump needs from our specialized lineup. The dij series of diffusion pumps is a 5stage oil diffusion pump with an improved gas throughput and stable high pressure in the range of 103 mbar.
Aug 31, 2014 diffusion pump is an oilbased vacuum pump, that is used for obtaining different levels of vacuum even high vacuum of 10 powered 9 pascal. The ulvac diffusion pumps have been designed for outstanding performance and extremely low running costs. Yet oil diffusion pumps require careful maintenance in order to sustain a high level of performance and maintain the integrity of the vacuum chamber. Product categories fomblin greases and fluids archive high. The main reason for this is that turbomolecular vacuum pumps. Diffusion vacuum pumps busch vacuum solutions united states. Operating diffusion pumps diffusion pump maintenance diffusion pump troubleshooting guide oil diffusion pumps are still a widely used type of high vacuum pump.
This is because they are relatively inexpensive, highly reliable, and very durable. Operation, maintenance and troubleshooting of oil diffusion pumps. Silicone based diffusion pump oil 1 gallon, same as dc704. Mar 08, 2007 oil diffusion pumps are still the most popular type of high vacuum pump because they are relatively inexpensive, highly reliable and very durable. The pumping speed ranges from 2,400 ls to 33,000 ls and has a operating range of 101 to 107 mbar. Since the chamber itself has no moving parts aside from the oil droplets, a vacuum diffusion pump can operate with stability over long periods. The pumping effect of these pumps is created through the diffusion of gases into an oil vapor stream.
Diffusion pump oil diffusion pump for various types of glass and metal working fluid, low saturated vapor pressure and good thermal stability and superior oxidation resistance, used in a variety of high vacuum industries, such as high vacuum coatingoptical coating, high vacuum smelting industry, high vacuum sintering brazing industrial vacuum distillation, the atomic energy industry. To ensure the satisfaction of our customers, our products are rigorously tested to ensure it reaches or exceeds all advertised specifications. We recommend that the period in which pump inlet pressure is above 150 millitorr be kept as short as possible. When your process requires a pressure below that of a mechanical pump or mechanical pump and roots pump combination a. Typical applications n vacuum coating n metallurgy n. Dij oil diffusion pumps are wearfree high vacuum pumps without wearing and moving components. Evp provide all kinds of rotary vacuum pumps such as direcdrive structure rotary vane vacuum pumps 2xz series, single stage oil sealed rotary vane vacuum pumps sv series, beltdrive rotary vane vacuum pumps 2xa series.
By combining edwards vapour diffusion pumps with either our. Agilent diffusion pumps offer high pumping speeds, high throughput, high tolerance forepressure. Oil for diffusion and ejector pumps ulvoil d series d11. For for a superior fluid for use where ultra high vacuum is required, please see our information on. Toshniwal deals with the tested and proven diffusion pumps from hsr ag took over from balzers ag in 2003 lichtenstein. They are often described as semiorganic due to their molecular structure, which is composed of siliconoxygen instead of carboncarbon bonds. Diffusion pump working principle diffusion pump oil by.
An oil diffusion pump is used to achieve higher vacuum lower pressure than is possible by use of positive displacement pumps alone. Thus a vacuum diffusion pump achieving a vacuum of 103 torr may also be said to have reached a vacuum of 1 micron. These pumps are offered with integral manual or pneumatic high vacuum. Evp provide all kinds of rotary vacuum pumps such as direcdrive structure rotary vane vacuum pumps 2xz series, single stage oilsealed rotary vane vacuum pumps sv series, beltdrive rotary vane vacuum pumps 2xa series. These pumps are very efficient and reliable and can be used to convey almost all gases even reactive gases. Maintenance and troubleshooting of oil diffusion pumps. At this point, the vacuum diffusion pump takes over to create. Gases on the high vacuum inlet side of the pump are captured in the jet vapor by. Although its use has been mainly associated within the high vacuum range down to 10. Oil diffusion pump vacuum pump evp vacuum solution. As the diffusion pump itself cannot maintain an outlet pressure, an additional forepump is required to maintain an outlet pressure of approximately 0. Oil diffusion pumps dij series online shop for vacuum. Although its use has been mainly associated within the highvacuum range down to 10. Oil diffusion vacuum pump ulk series ulvac s diffusion pumps ulk series have been developed not only for superior performance, but also for extremely low operating cost.
A rotary vane vacuum pump is an oilsealed rotary displacement pump. Oil diffusion pumps are characterized by superior vacuum performance data and are welladapted as reliable components in medium vacuum and high vacuum systems due to their rugged design. This article will explain practical steps that can be taken to ensure optimal performance of oil. Diffusion pump fluids inland vacuum industries, inc. Oil diffusion pump ulvac has drawn on a wealth of experience in evacuation technology to redesign the oil diffusion pumps meeting the demands of a new era. Oil diffusion pumps from leybold are ideally suited for industrial high vacuum applications. The pump has no moving parts which may be corroded by the acidic nature of the material being pumped. At the bottom, you can see the heaters that sit just below the oil. These vapor jet pumps are one of the oldest and most reliable ways to create a vacuum. The heated oil is ejected from the jet assembly at supersonic speeds and the process gas molecules are entrained in the oil jet flow and transferred through the pump body by the heavier oil molecules momentum. Diffusion pump oil diffusion pump for various types of glass and metal working fluid, low saturated vapor pressure and good thermal stability and superior oxidation resistance, used in a variety of high vacuum industries, such as high vacuum coatingoptical coating, high vacuum smelting industry, highvacuum sintering brazing industrial vacuum distillation, the atomic energy industry. While diffusion pumps are probably the most costeffective method of creating a high vacuum, there are limitations that make it not suitable for some applications.
In this system the oil is boiled by a heating with a. Oil diffusion vacuum pump ulk series oil diffusion pump. Educational guide to vacuum coating processing the oil diffusion pump often called the diff pump or dp is probably the most widely used highvacuum pump. Generally speaking, diffusion pumps can attain vacuums between 10e6 to 10e10 torr depending on the size of the pump as well as the type of diffusion pump oil used. Diffusion pump oil recycling silicone recycling silicone.
In practice, to reduce specimen contamination, a diffusion pump oil of low vapor pressure should be employed. The use of lowvapourpressure oils rather than mercury in diffusion pumps was. The oil diffusion pumps can reach a vacuum of 500 ls. When the oil view diffusion pump oil selection online becomes hot enough to vaporize, the oil vapors rise up the center of the pump and exit the nozzles at a downward angle. With the proper choice of motive fluids, traps, baffles, and valves, diffusion pumps can be used in a wide variety of applications and over pressure ranges from 1 x 103 torr to 2 x 1011 torr key features of agilent diffusion pumps include. Oil diffusion pump controls vacuum furnace engineering. Because of its simplicity, high performance and low initial cost, the diffusion pump is the primary industrial high vacuum pumping mechanism. As stated earlier, there are no moving parts in a diffusion pump. They excel with superior vacuum performance and are reliable components in medium vacuum and high vacuum systems with a fit and form retrofit capability.
The oildiffusion pumps can reach a vacuum of 500 ls. Upon collision, the positive gas ions react with the cathode, combining chemically with a cathode atom. The design solution unfolded as a merger of three interrelated concepts. Instead, an ancillary mechanical roughing pump or forepump, capable of a modest level of pumping, first brings the pressure inside the vacuum diffusion chamber down to about 103 torr. Oil diffusion pumps remain in popular use in the vacuum heat treating industry, possibly one of the few applications remaining for this type of high vacuum pump in the western world. Agilent diffusion pumps offer high pumping speeds, high throughput, high tolerance forepressure, excellent backstreaming characteristics, low ultimate pressure, and longterm reliability.
The ksm200 is a three stage, high vacuum 103 to 104 torr range vapor pump designed for heavy gas load applications such as in vacuum distillation, evaporation, vacuum arc melting, freeze drying, impregnation and casting of metals. A vacuum diffusion pump cannot begin its work with full. Performance of lion diffusion pump oil 11 corelationship between ultimate pressure temperature 1 pressure temperature relationship of lion diffusion pump oil a method. A vacuum diffusion pump cannot begin its work with full atmospheric pressure inside the chamber. The main reasons for their continued use are their longevity the lack of other options. The difference is that the diffusion pump works in the high vacuum area, and its working pressure range is 102106 pa. The flexibility inherent in our line of diffusion pump fluids will allow the user to incorporate the same oil in both high vacuum and mechanical pump units. The pumping speed ranges from 2,400 ls to 33,000 ls and has a operating range of 101 to 107 mbar more. Basics of maintenance and troubleshooting of vacuum authors. Vhs6, 6 asa, kf50, 120 vac, single phase, download pdf. Ksm 200 oil diffusion ejector pump myers vacuum molecular.